SYNTHESIS OF CARBON NANOSTRUCTURES ON NICKEL FILMS BY OXYGEN-ACETYLENE COMBUSTION FLAME
Keywords:
кислородно-ацетиленовая горелка, углеродные наноструктуры, сканирующая электронная микроскопия, никелевая пленка, комбинационное рассеяние света.Abstract
In this work arepresented results of experiments on the synthesis of carbon nanostructures by the method of oxygen-acetylene torch on the surface of pre-deposited nickel thin films. The influence of the distance from the nozzle of torch to the substrate on the structure formation was investigated. Studies of the samples by Raman scattering showed that depending on the experimental conditions, the synthesis of mono- and multilayer graphenes occurred. Besides, the results of Raman spectroscopy showed the possibility of synthesis of carbon nanotubes or nanofibers by the method of oxygen-acetylene torch.
References
(1) А.В. Елецкий, И.М. Искандарова, А.А. Книжник, Д.Н. Красиков. Графен: методы получения и теплофизические свойства. Успехи физических наук, Том 181, № 3, 2011, с. 233-268.
(2) Е.Д. Грайфер, В.Г. Макотченко, А.С. Назаров, С.-Дж. Ким, В.Е. Федоров. Графен: химические подходы к синтезу и модифицированию. Успехи химии, 80, (8), 2011, с. 784-804.
(3) Diamond thin films: a 21st-century material. P.W. May, Phil.Trans. R. Soc. Lond., A 358, (2000), pp. 473-495. https://doi.org/10.1098/rsta.2000.0542
(4) Е.С. Меркибаев, Regina Fuchs, Б.З. Мансуров, Б.С. Медянова, А.К. Кенжегулов, А. Толеген, Б.Т. Лесбаев, Б.А. Алиев, Структура и механические свойства углеродных пленок, полученных методом кислородно ацетиленовой горелки. Горение и плазмохимия, №3, 2013 г., с. 85-90.
(5) Saito R., Hofmann M., Dresselhaus G., Jorio A., Dresselhaus M.S. Raman spectroscopy of graphene and carbon nanotubes. http://www.tandfonline.com/loi/tadp20
(6) Волкова Я.Б., Резчикова Е.В., Шахнов В.А. Методы получения и результаты исследования свойств графена // Вестник МГТУ им. Н.Э. Баумана. Спец. выпуск "Наноинженерия". – 2013. - №6. – C.6.
(7) Zheng Yan, Andrew R. Barron. Characterization of graphene by Raman spectroscopy // Режим доступа: http://cnx.org/content/m34667/1.2/
(8) Keith B. Dillon, David W. H. Rankin. Spectroscopic Properties of Inorganic and Organometallic Compounds // Royal Society of Chemistry. – 20 December, 2000. – Vol.33 – P. 311.
(9) Feng-Ming Liu, Bin Ren, Jia-Wei Yan, Bing-Wei Mao, Zhong-Qun Tian. Initial Oxidation Processes on Hydrogenated Silicon Surfaces Studied by In Situ Raman Spectroscopy // Journal of The Electrochemical Society. – 2002 – Vol.149 – P. 95-99. https://doi.org/10.1149/1.1426400
(10) Ihtesham ur Rehman, Zanyar Movasaghi, Shazza Rehman. Vibrational Spectroscopy for Tissue Analysis // Series in Medical Physics and Biomedical Engineering. – 2012 – P.281.
(11) Bo Zeng, Min Gao, Shenghua Liu, Taisong Pan, Zhenlong Huang, and Yuan Lin. Thermal chemical vapor deposition of layered aligned carbon-nanotube films separated by graphite layers // Physica status solidi (a). – 2013. – Vol.210 – №6, P. 1128–1132. https://doi.org/10.1002/pssa.201228579
(12) Characterization of carbon nanotubes by Raman spectroscopy. S. Costa, E. Borowiak- Palen, M. Kruszyńska, A. Bachmatiuk, R. J. Kaleńczuk // Materials Science-Poland. – 2008 – Vol. 26 – №2 – P. 1-9.
