Synthesis of nanomaterials in a flame
DOI:
https://doi.org/10.18321/cpc21(1)17-27Keywords:
nanomaterials, fullerenes, nickel nanoparticles, grapheneAbstract
The article presents the results of experimental studies on the synthesis of fullerenes, nickel oxide nanoparticles and graphenes in a flame, which were carried out at the Institute of Combustion Problems. The article presents the conditions for the synthesis of C60 fullerenes in a pre-mixed benzene-oxygen flame with the application of an electric field and a pressure of 40 Torr. The maximum yield of C60 fullerenes up to 15% was found when a glow discharge was applied to the flame using a ring-plane interelectrode system. The conditions for the synthesis of nickel oxide nanoparticles in a diffusion propane-oxygen counterflow flame have been revealed, and it has been established that by varying the treatment time of the nichrome wire from 5 sec to 2 min, it is possible to control the size of the resulting nickel oxide nanoparticles from 70 to 700 nanometers, while the subsequent flame treatment is more than 2 min does not lead to appreciable changes in size. The conditions for the synthesis of graphenes in a coaxial flame have
been determined, and it has been established that by organizing coaxial combustion, by changing the types of fuels, it is possible to achieve conditions for obtaining graphenes with a given number of layers.
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